Technology Process of C31H28BF2N5O3
There total 14 articles about C31H28BF2N5O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 19.5h;
DOI:10.1021/ja5020053
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / dichloromethane / 19 h / 20 °C
1.2: 0.33 h
1.3: 0.17 h / 0 °C
2.1: Schwartz's reagent / tetrahydrofuran / 0.08 h / 20 °C
3.1: acetic acid / dichloromethane / 2 h / 20 °C
3.2: 0.17 h
4.1: hydrogenchloride / ethyl acetate / 19.5 h / 20 °C
With
hydrogenchloride; Schwartz's reagent; acetic acid; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ja5020053
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Schwartz's reagent / tetrahydrofuran / 0.08 h / 20 °C
2.1: acetic acid / dichloromethane / 2 h / 20 °C
2.2: 0.17 h
3.1: hydrogenchloride / ethyl acetate / 19.5 h / 20 °C
With
hydrogenchloride; Schwartz's reagent; acetic acid;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ja5020053