N-(Benzyloxycarbonyl)valine N-methoxyamide

Base Information

Chemical Name:N-(Benzyloxycarbonyl)valine N-methoxyamide
CAS No.:145276-03-5
Molecular Formula:C₁₄H₂₀N₂O₄
Molecular Weight:280.324
Hs Code.:

Synonyms:N-(Benzyloxycarbonyl)valine N-methoxyamide

Suppliers and Price of N-(Benzyloxycarbonyl)valine N-methoxyamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(Benzyloxycarbonyl)valine N-methoxyamide

Chemical Property:

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Technology Process of N-(Benzyloxycarbonyl)valine N-methoxyamide

There total 3 articles about N-(Benzyloxycarbonyl)valine N-methoxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 67-62-9
O-Methylhydroxylamin

: 1149-26-4,1685-33-2,92077-76-4,3588-63-4
N-benzyloxycarbonylvaline

: 145276-03-5
N-(Benzyloxycarbonyl)valine N-methoxyamide

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; water; for 5h; Ambient temperature;
DOI:10.1021/jo00051a019

Reference yield:

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 145276-03-5
N-(Benzyloxycarbonyl)valine N-methoxyamide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 4N NaOH / H₂O / 0 deg C to r.t., 1 h

2: 71 percent / dicyclohexylcarbodiimide / dioxane; H₂O / 5 h / Ambient temperature

With sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; water;
DOI:10.1021/jo00051a019

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 145276-03-5
N-(Benzyloxycarbonyl)valine N-methoxyamide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 4N NaOH / H₂O / 0 deg C to r.t., 1 h

2: 71 percent / dicyclohexylcarbodiimide / dioxane; H₂O / 5 h / Ambient temperature

With sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; water;
DOI:10.1021/jo00051a019