2,6-diethyl-4-fluorobenzenamine

Base Information

Chemical Name:2,6-diethyl-4-fluorobenzenamine
CAS No.:117336-04-6
Molecular Formula:C₁₀H₁₄FN
Molecular Weight:167.226
Hs Code.:

Synonyms:2,6-diethyl-4-fluorobenzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-diethyl-4-fluorobenzenamine

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Technology Process of 2,6-diethyl-4-fluorobenzenamine

There total 3 articles about 2,6-diethyl-4-fluorobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 97-94-9
triethyl borane

: 344-18-3
2,6-dibromo-4-fluoroaniline

: 117336-04-6
2,6-diethyl-4-fluorobenzenamine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In hexane; N,N-dimethyl-formamide; at 50 ℃; for 22h;
DOI:10.1021/jm990170q

Reference yield:

: 371-40-4
4-fluoroaniline

: 117336-04-6
2,6-diethyl-4-fluorobenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.04 g / Br₂ / CH₂Cl₂

2: 64 percent / (dppf)PdCl₂, CsCO₃ / dimethylformamide; hexane / 22 h / 50 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; bromine; In hexane; dichloromethane; N,N-dimethyl-formamide; 1: Bromination / 2: ethylation;
DOI:10.1021/jm990170q