3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Base Information

Chemical Name:3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole
CAS No.:1269646-54-9
Molecular Formula:C₁₄H₁₉BrFN₃OSi
Molecular Weight:372.312
Hs Code.:

Synonyms:3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

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Chemical Property of 3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

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Technology Process of 3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

There total 9 articles about 3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228014-45-6
5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 73183-34-3
bis(pinacol)diborane

: 1269646-54-9
3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

: 1269646-55-0
5-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: 5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

(2-trimethylethylsilylethoxy)methyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h;

bis(pinacol)diborane; With potassium acetate; (diphenylphosphin)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; at 20 - 90 ℃; for 92.5h; Inert atmosphere;

Reference yield:

: 1228014-45-6
5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1269646-54-9
3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

: 1269646-55-0
5-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: 5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

(2-trimethylethylsilylethoxy)methyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h;

Reference yield:

: 1228014-45-6
5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole

: 1269646-21-0
(S)-3-(3-bromopyrazolo[1,5-a]pyrimidin-5-yl)-4-isopropyloxazolidin-2-one

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 73183-34-3
bis(pinacol)diborane

: 1269646-54-9
3-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

: 1269646-55-0
5-(4-bromo-2-fluorophenyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-1,2,4-triazole

Guidance literature:: 5-(4-bromo-2-fluorophenyl)-1H-1,2,4-triazole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

(2-trimethylethylsilylethoxy)methyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h;

(S)-3-(3-bromopyrazolo[1,5-a]pyrimidin-5-yl)-4-isopropyloxazolidin-2-one; bis(pinacol)diborane;