HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

Base Information

Chemical Name:HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe
CAS No.:1295578-90-3
Molecular Formula:C₂₇H₄₄N₄O₅*ClH
Molecular Weight:541.131
Hs Code.:

Synonyms:HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

Chemical Property:

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Technology Process of HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

There total 9 articles about HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1295578-87-8
Boc-Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

: 1295578-90-3
HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c0ob01047b

Reference yield:

: 4-[1'-(2'',2'',6'',6''-tetramethyl-1''-piperidinyloxy)ethyl]benzoic acid

: 1295578-90-3
HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: hydrogenchloride / methanol / 16 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1039/c0ob01047b

Reference yield:

: 178625-97-3
1-[1-(4-bromophenyl)ethoxy]-2,2,6,6-tetramethylpiperidine

: 1295578-90-3
HCl*Lys(4-[1-{2,2,6,6-tetramethylpiperidin-1-yloxy}ethyl]benzoyl)-Gly-OMe

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.33 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

1.3: 20 °C

2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / methanol / 16 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; tert.-butyl lithium; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; pentane;
DOI:10.1039/c0ob01047b