Technology Process of C11H10N4S
There total 3 articles about C11H10N4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
toluene;
at 0 - 23 ℃;
Inert atmosphere;
DOI:10.1016/j.molcatb.2014.05.007
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium; iodine / diethyl ether / Reflux; Inert atmosphere
1.2: Cooling with ice; Reflux
2.1: immobilized lipase B from Candida antarctica; vinyl acetate / toluene / 6 h / 23 °C / Molecular sieve; Resolution of racemate; Enzymatic reaction
3.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0 - 23 °C / Inert atmosphere
With
vinyl acetate; immobilized lipase B from Candida antarctica; diphenyl phosphoryl azide; iodine; magnesium; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
diethyl ether; toluene;
1.2: |Grignard Reaction;
DOI:10.1016/j.molcatb.2014.05.007
- Guidance literature:
-
Multi-step reaction with 2 steps
1: immobilized lipase B from Candida antarctica; vinyl acetate / toluene / 6 h / 23 °C / Molecular sieve; Resolution of racemate; Enzymatic reaction
2: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0 - 23 °C / Inert atmosphere
With
vinyl acetate; immobilized lipase B from Candida antarctica; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
toluene;
DOI:10.1016/j.molcatb.2014.05.007
