(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

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Chemical Name:(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide
CAS No.:1054645-95-2
Molecular Formula:C₃₅H₅₀N₆O₅
Molecular Weight:634.819
Hs Code.:

Synonyms:(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

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Chemical Property of (3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

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Technology Process of (3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

There total 6 articles about (3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58521-49-6
(3S,4S)-4-(tert-butoxycarbonylamino)-3-hydroxy-6-methylheptanoic acid

: 1054645-95-2
(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / HOBt, DCCI / CH₂Cl₂ / 1) 0 deg C, 2) r.t., overnight

2: 4 M HCl / dioxane

3: 23 percent / HOBt, DCCI / CH₂Cl₂ / 1) 0 deg C, 2) r.t., overnight

4: 4 M HCl / dioxane

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;

Reference yield:

: 67010-43-9
(3S,4S)-ethyl 4-(tert-butoxycarbonylamino)-3-hydroxy-6-methylheptanoate

: 1054645-95-2
(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1: 1 M NaOH / methanol

2: 70 percent / HOBt, DCCI / CH₂Cl₂ / 1) 0 deg C, 2) r.t., overnight

3: 4 M HCl / dioxane

4: 23 percent / HOBt, DCCI / CH₂Cl₂ / 1) 0 deg C, 2) r.t., overnight

5: 4 M HCl / dioxane

With hydrogenchloride; sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 1055034-47-3
(3S,4S)-4-Amino-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

: 1054645-95-2
(3S,4S)-4-[(S)-2-Amino-3-(1-benzyl-1H-imidazol-4-yl)-propionylamino]-3-hydroxy-6-methyl-heptanoic acid [5-(4-methoxy-benzylcarbamoyl)-pentyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / HOBt, DCCI / CH₂Cl₂ / 1) 0 deg C, 2) r.t., overnight

2: 4 M HCl / dioxane

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;