(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

Base Information

Chemical Name:(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne
CAS No.:628293-07-2
Molecular Formula:C₂₅H₃₈O₃
Molecular Weight:386.575
Hs Code.:

Synonyms:(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

Suppliers and Price of (6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

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Chemical Property of (6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

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Technology Process of (6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

There total 11 articles about (6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: Thiocarbonic acid O-((E)-(3R,6R,7R)-12-benzyloxy-6-methoxymethoxy-1,3,5,7-tetramethyl-dodec-4-en-8-ynyl) ester O-phenyl ester

: 628293-07-2
(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; Heating;
DOI:10.1021/jo0496042

Reference yield: 16.0%

: 628293-06-1
(E)-(4R,7R,8R)-13-benzyloxy-7-methoxymethoxy-4,6,8-trimethyltridec-5-en-9-yn-2-one

: 628293-07-2
(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

Guidance literature:: (E)-(4R,7R,8R)-13-benzyloxy-7-methoxymethoxy-4,6,8-trimethyltridec-5-en-9-yn-2-one; With toluene-4-sulfonic acid hydrazide;

With sodium cyanoborohydride;
DOI:10.1021/jo0496042

Reference yield:

: 725724-80-1
(2RS,4R,5E,7R,8R)-13-benzyloxy-7-methoxymethoxy-4,6,8-trimethyltridec-5-en-9-yn-2-ol

: 628293-07-2
(6R,7R,8E,10R)-1-benzyloxy-7-methoxymethoxy-6,8,10-trimethyltridec-8-en-4-yne

Guidance literature:: Multi-step reaction with 2 steps

1: i-Pr₂NEt / CH₂Cl₂ / 2 h / 0 °C

2: 291 mg / LiAlH₄ / tetrahydrofuran / 3 h / Heating

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0496042