N-phenyl-pentamethylenediamine

Base Information

• Chemical Name: N-phenyl-pentamethylenediamine
• CAS No.: 100051-07-8
• Molecular Formula: C₁₁H₁₈N₂
• Molecular Weight: 178.277

Synonyms:N-phenyl-pentamethylenediamine

Chemical Property of N-phenyl-pentamethylenediamine

Chemical Property:

Purity/Quality:

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Technology Process of N-phenyl-pentamethylenediamine

There total 8 articles about N-phenyl-pentamethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

5-(phenylamino)valeronitrile (13659-00-2) → N-phenyl-pentamethylenediamine (100051-07-8)

Guidance literature:

With borane; In tetrahydrofuran; for 1h; Reflux;

DOI:10.1055/s-0028-1087817

Reference yield: 74.0%

N-benzoyl-N'-phenylpentamethylenediamine → N-phenyl-pentamethylenediamine (100051-07-8)

Guidance literature:

With sulfuric acid; In water; at 150 ℃; for 0.133333h; Microwave irradiation;

DOI:10.1016/j.tetlet.2010.07.075

Reference yield: 73.0%

5-azido-pentanoic acid phenylamide (879216-05-4) → N-phenyl-pentamethylenediamine (100051-07-8)

Guidance literature:

With diborane; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2011.01.088

upstream raw materials:

5-(phenylamino)valeronitrile

δ-chlorovaleronitrile

aniline

5-azido-pentanoic acid phenylamide

Downstream raw materials:

N-formyl-N'-phenyl-1,5-diaminopentane

1-phenyl-1,4,5,6,7,8-hexahydro-1,3-diazocine

3-methyl-1,2-diphenyl-1,4,5,6,7,8-hexahydro-1,3-diazocinium iodide

C₁₉H₂₂ClN₂⁽¹⁺⁾*I^(1-)

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