[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

Base Information

Chemical Name:[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid
CAS No.:852948-65-3
Molecular Formula:C₁₆H₁₈Cl₂NO₅P
Molecular Weight:406.202
Hs Code.:

Synonyms:[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

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Chemical Property of [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

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Technology Process of [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

There total 3 articles about [3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₀Cl₂NO₅P

: 852948-65-3
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 16.1667h;

Reference yield:

: C₂₂H₂₈Cl₂NO₇P

: 852948-65-3
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm800824d

Reference yield:

: 155891-93-3
(3,5-Dichloro-4-hydroxy-phenyl)-carbamic acid tert-butyl ester

: 852948-65-3
[3,5-dichloro-4-(4'-hydroxy-3'-isopropylphenoxy)phenylamino]methylphosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper; triethylamine / dichloromethane / 14 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 2 h / 20 °C

3.1: trimethylsilyl bromide / dichloromethane / 16 h / 0 - 20 °C

4.1: boron tribromide / dichloromethane / 16.17 h / -78 - 20 °C

With trimethylsilyl bromide; boron tribromide; copper; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;