1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

Base Information

Chemical Name:1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate
CAS No.:869496-55-9
Molecular Formula:C₁₅H₂₀O₈
Molecular Weight:328.319
Hs Code.:

Synonyms:1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

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Chemical Property of 1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

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Technology Process of 1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

There total 5 articles about 1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 693245-36-2
(3S,4S,5R,6S,7R)-4,5,6,7-tetrahydroxy-1-oxaspiro[2,5]octane

: 869496-55-9
1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

Guidance literature:: (3S,4S,5R,6S,7R)-4,5,6,7-tetrahydroxy-1-oxaspiro[2,5]octane; With hydrogen iodide; In acetic acid;

acetic anhydride;

With acetic acid; zinc; Further stages.;
DOI:10.1039/b314795a

Reference yield: 85.0%

: 942132-21-0
Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

: 869496-55-9
1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

Guidance literature:: With acetic acid; zinc; for 2h; Heating;
DOI:10.1081/CAR-200064653

Reference yield:

: 488-76-6
(-)-viburnitol

: 869496-55-9
1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / Gluconobacter sp. AB₁₀₂₇₇; aq. K₂HPO₄; (NH₄)2SO₄ / H₂O / 72 h / 27 °C / pH 7.0

2.1: 44 percent / methanol; diethyl ether

3.1: hydroiodic acid / acetic acid

3.3: 100 percent / Zn; AcOH

With ammonium sulfate; dipotassium hydrogenphosphate; Gluconobacter sp. AB₁₀₂₇₇; hydrogen iodide; In methanol; diethyl ether; water; acetic acid;
DOI:10.1039/b314795a