Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

Base Information

Chemical Name:Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester
CAS No.:942132-21-0
Molecular Formula:C₁₇H₂₃IO₁₀
Molecular Weight:514.268
Hs Code.:

Synonyms:Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

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Technology Process of Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

There total 1 articles about Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 64-19-7,77671-22-8
acetic acid

: 693245-36-2
(3S,4S,5R,6S,7R)-4,5,6,7-tetrahydroxy-1-oxaspiro[2,5]octane

: 942132-21-0
Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

Guidance literature:: With hydrogen iodide; at 20 ℃;
DOI:10.1081/CAR-200064653

Reference yield: 85.0%

: 942132-21-0
Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

: 869496-55-9
1L-(1,3/2,4)-5-methylene-1,2,3,4-cyclohexanetetrol tetra-acetate

Guidance literature:: With acetic acid; zinc; for 2h; Heating;
DOI:10.1081/CAR-200064653

Reference yield:

: 942132-21-0
Acetic acid (1S,2R,4R,5S,6R)-2,4,5,6-tetraacetoxy-2-iodomethyl-cyclohexyl ester

: C₂₀H₂₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / Zn; acetic acid / 2 h / Heating

2: NaOMe / methanol

3: TsOH*H₂O / dimethylformamide / 20 °C

4: 35 percent / 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide hydrochloride; Et₃N; 4-(dimethylamino)pyridine / CH₂Cl₂ / -30 - 20 °C

5: 100 percent / pyridine; 4-(dimethylamino)pyridine

6: 15 percent / LiCl; triethylamine / dimethylformamide / 85 °C

With pyridine; dmap; sodium methylate; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium chloride; zinc; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-200064653