(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

Base Information

Chemical Name:(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane
CAS No.:198023-07-3
Molecular Formula:C₅₁H₈₄SeSi₆Sn
Molecular Weight:1063.41
Hs Code.:

Synonyms:(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

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Chemical Property of (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

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Technology Process of (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

There total 4 articles about (2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 198023-03-9
5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-[2,6-bis(2-isopropylphenyl)phenyl]-1,2,3,4,5-tetraselenastannolane

: 198023-07-3
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

Guidance literature:: With triphenylphosphine; In hexane; byproducts: Ph3P=Se; mixt. (3 equiv. PPh3) refluxing under Ar for 2 h, Ph3P=Se filtration off, solvent removal;
DOI:10.1080/10426509708046793

Reference yield: 84.0%

: 198023-02-8
(C₆H₂(CH(CH₃CH₂)2)3)(C₆H₂(CH(Si(CH₃)3)2)3)SnSe₄

: 198023-07-3
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

Guidance literature:: With triphenylphosphine; In hexane; byproducts: Ph3PSe; (Ar); 3 equiv. of triphenylphospine, reflux (2 h); filtn., evapn.;
DOI:10.1021/ja972221j

Reference yield:

: 198023-04-0
2'-iodo-2,2''-diisopropyl-1,1':3',1''-terphenyl

: 198023-07-3
(2,4,6-tris[Bis(trimethylsilyl)methyl]phenyl)(2,2''-diisopropyl-m-terpheny-2'-yl)monoselenastannirane

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuLi / diethyl ether; pentane; tetrahydrofuran

2: PPh₃ / hexane

With t-BuLi; PPh₃; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/ja048453h