(η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate

Base Information

Chemical Name:(η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate
CAS No.:664334-88-7
Molecular Formula:C₁₈H₂₅Ru*F₆P
Molecular Weight:487.431
Hs Code.:

Synonyms:(η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate

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Technology Process of (η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate

There total 1 articles about (η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: sodium hexaflorophosphate

: 14898-67-0
ruthenium trichloride hydrate

: 4045-44-7
1,2,3,4,5-pentamethylcyclopentadiene

: 100-41-4,27536-89-6
ethylbenzene

: 664334-88-7
(η5-pentamethylcyclopentadienyl)(η6-ethylbenzene)ruthenium hexafluorophosphate

Guidance literature:: With Zn; In ethanol; (Ar); Zn added to soln. of Ru salt in ethanol, treated with arene, stirred for 10 min at room temp., treated with Cp*H and NaPF6, stirred for 1 d at room temp., 2 d at 60°C; isooctane added, filtered (Al2O3), concd., filtered (aminopropyl SiO2 eluent isooctane/EtOH 1:1), treated with MeOH, extd.(isooctane twice), extd.(H2O/MeOH 1:1), polar phase evapd., extd.(CH2Cl2), recrystd.(H2O/isopropanol), elem. anal.;
DOI:10.1002/ejic.200200579