N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

Base Information

• Chemical Name: N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide
• CAS No.: 260360-37-0
• Molecular Formula: C₈₉H₁₁₃N₁₉O₂₂
• Molecular Weight: 1800.99

Synonyms:N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

Chemical Property of N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

Chemical Property:

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Technology Process of N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

There total 2 articles about N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide (260360-36-9) + methyl iodide (74-88-4) → N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide (260360-37-0) + N-methyl-N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide;

DOI:10.1016/S0008-6215(99)00185-8

Reference yield:

N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide (260360-36-9) + methyl iodide (74-88-4) → N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide (260360-37-0)

Guidance literature:

With silver(l) oxide;

DOI:10.1016/S0008-6215(99)00185-8

Reference yield: 81.0%

N-(2,2-dimethoxyethyl)-6-[2-O-methyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide (260360-37-0) → N-(2,2-dimethoxyethyl)-6-[4-amino-3-O-benzyl-4,6-dideoxy-2-O-methyl-α-D-mannopyranosyl-(1->2)-tetrakis(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

Guidance literature:

With hydrogen sulfide; In pyridine; water; at 40 ℃;

DOI:10.1016/S0008-6215(99)00185-8

upstream raw materials:

N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-tetrakis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

methyl iodide

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