((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

Base Information

Chemical Name:((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride
CAS No.:68426-76-6
Molecular Formula:C₂₇H₂₄N₂P*Cl
Molecular Weight:442.928
Hs Code.:

Synonyms:((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

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Chemical Property of ((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

Chemical Property:

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Technology Process of ((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

There total 4 articles about ((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4760-35-4
2-chloromethyl-1-methyl-1H-benzimidazole

: 603-35-0
triphenylphosphine

: 68426-76-6
((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

Guidance literature:: In 1,4-dioxane; at 100 ℃;
DOI:10.1021/acs.organomet.0c00618

Reference yield:

: 4760-34-3
N-methyl-1,2-phenylenediamine

: 68426-76-6
((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / Reflux

2: toluene / Reflux

With hydrogenchloride; In water; toluene;
DOI:10.1021/ja404422z

Reference yield:

: 25148-68-9
N-methylbenzene-1,2-diamine dihydrochloride

: 68426-76-6
((1-methyl-1H-benzo[d]imidazol-2-yl)methyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / Reflux

1.2: 3 h

2.1: 1,4-dioxane / 100 °C

With hydrogenchloride; In 1,4-dioxane; water;
DOI:10.1021/acs.organomet.0c00618