allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside

Base Information

• Chemical Name: allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside
• CAS No.: 78835-49-1
• Molecular Formula: C₈₈H₁₅₅ClN₂O₁₄
• Molecular Weight: 1500.66

Synonyms:allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside

Chemical Property of allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside

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Technology Process of allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside

There total 1 articles about allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

allyl 2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside (78835-47-9) + 2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline (78835-46-8) → allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside (78835-49-1)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 70 ℃; for 8h;

DOI:10.1016/S0008-6215(00)80408-5

Reference yield: 90.0%

allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside (78835-49-1) + n-hexadecanoyl chloride (112-67-4) → allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3,4-di-O-palmitoyl-β-D-glucopyranoside (78835-50-4)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1016/S0008-6215(00)80408-5

upstream raw materials:

allyl 2-deoxy-2-palmitamido-3-O-palmitoyl-β-D-glucopyranoside

2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

Downstream raw materials:

allyl O-(3-O-benzyl-4-O-chloroacetyl-2-deoxy-2-palmitamido-6-O-palmitoyl-β-D-glucopyranosyl)-(1<*>6)-2-deoxy-2-palmitamido-3,4-di-O-palmitoyl-β-D-glucopyranoside

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