C₃₂H₄₈O₅Si

Base Information

Chemical Name:C₃₂H₄₈O₅Si
CAS No.:1207384-17-5
Molecular Formula:C₃₂H₄₈O₅Si
Molecular Weight:540.816
Hs Code.:

C<sub>32</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:C₃₂H₄₈O₅Si

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Chemical Property of C₃₂H₄₈O₅Si

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Technology Process of C₃₂H₄₈O₅Si

There total 19 articles about C₃₂H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1207384-16-4
C₃₆H₅₂O₇Si

: 1207384-17-5
C₃₂H₄₈O₅Si

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/ol902711b

Reference yield:

: C₂₆H₃₀O₄Se

: 1207384-17-5
C₃₂H₄₈O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide / dichloromethane / 0.25 h / Inert atmosphere

2: caesium carbonate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; caesium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo501122k

Reference yield:

: 89922-82-7
3-(tert-butyldimethylsilanyloxy)propionaldehyde

: 1207384-17-5
C₃₂H₄₈O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: dichloromethane / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

6.1: caesium carbonate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisobutylaluminium hydride; caesium carbonate; Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; toluene; 1.1: |Wittig Olefination / 3.1: |Dess-Martin Oxidation / 5.1: |Dess-Martin Oxidation;
DOI:10.1021/jo501122k