2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

Base Information

Chemical Name:2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane
CAS No.:219646-55-6
Molecular Formula:C₃₉H₄₅O₈PS
Molecular Weight:704.821
Hs Code.:

Synonyms:2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

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Technology Process of 2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

There total 1 articles about 2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4132-28-9,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4291-69-4
2,3,4,6-tetra-O-benzyl-α-D-galactopyranose

: 4090-61-3
2-Hydroxy-5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane triethylammonium salt

: 219646-55-6
2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; for 24h; Yield given;
DOI:10.1515/znb-1998-1107

Reference yield: 74.0%

: 219646-55-6
2-S-(2,3,4,6-Tetra-O-benzyl-α-D-galactopyranosyl)-2-oxo-5,5-dimethyl-1,3,2-dioxaphosphorinane

: 762-72-1
allyl-trimethyl-silane

: 82659-55-0
3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1515/znb-2002-0217