4-Methylbenzoylsulfenyl iodide

Base Information

• Chemical Name: 4-Methylbenzoylsulfenyl iodide
• CAS No.: 80461-75-2
• Molecular Formula: C₈H₇IOS
• Molecular Weight: 278.113

Synonyms:4-Methylbenzoylsulfenyl iodide

Chemical Property of 4-Methylbenzoylsulfenyl iodide

Chemical Property:

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Technology Process of 4-Methylbenzoylsulfenyl iodide

There total 3 articles about 4-Methylbenzoylsulfenyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

CH3C6H4COSHgC6H5 (79293-02-0) → 4-Methylbenzoylsulfenyl iodide (80461-75-2)

Guidance literature:

With iodine; In methanol; chloroform; 1) 1 h, room temperature, 2) -60 deg C, 1 h;

Reference yield: 40.0%

Silver 4-methylthiobenzoate (87662-83-7) → 4-Methylbenzoylsulfenyl iodide (80461-75-2)

Guidance literature:

With iodine; In methanol; dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1055/s-1983-30420

Reference yield:

C28H24O2S2Sn (88584-79-6) → 4-Methylbenzoylsulfenyl iodide (80461-75-2)

Guidance literature:

With iodine; In hexane; for 0.5h; Ambient temperature;

DOI:10.1055/s-1983-30525

upstream raw materials:

CH₃C₆H₄COSHgC₆H₅

Silver 4-methylthiobenzoate

C₂₈H₂₄O₂S₂Sn

Downstream raw materials:

4-Methylbenzoyl(thiobenzoyl)disulfid

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