3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

Base Information

Chemical Name:3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon
CAS No.:98909-53-6
Molecular Formula:C₂₁H₂₃ClO₅
Molecular Weight:390.864
Hs Code.:

Synonyms:3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

Chemical Property:

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Technology Process of 3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

There total 3 articles about 3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98-01-1
furfural

: 98909-44-5
1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

: 98909-53-6
3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

Guidance literature:: With triethylamine; HEMET(+) Br(-); In ethanol; at 80 ℃; for 16h;

Reference yield:

: 53842-12-9
1-(p-chlorophenyl)-1,4-pentanedione

: 98909-53-6
3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / p-Me-C₆H₄-SO₃H / CCl₄ / Heating

2: 1.) Bu₄N(+) I(-), KOH, 2.) DCC, CuCl / 1.) THF, H₂O, r.t., 2.) THF, 20 h, reflux

3: 78 percent / Et₃N / HEMET(+) Br(-) / ethanol / 16 h / 80 °C

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide; copper(l) chloride; HEMET(+) Br(-); In tetrachloromethane; ethanol;

Reference yield:

: 98909-39-8
1-(4-Chlorphenyl)-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

: 98909-53-6
3-(4-Chlorbenzoyl)-1-(2-furyl)-4-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-butanon

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₄N(+) I(-), KOH, 2.) DCC, CuCl / 1.) THF, H₂O, r.t., 2.) THF, 20 h, reflux

2: 78 percent / Et₃N / HEMET(+) Br(-) / ethanol / 16 h / 80 °C

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; triethylamine; dicyclohexyl-carbodiimide; copper(l) chloride; HEMET(+) Br(-); In ethanol;