1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Base Information

Chemical Name:1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon
CAS No.:98909-44-5
Molecular Formula:C₁₆H₁₉ClO₃
Molecular Weight:294.778
Hs Code.:

Synonyms:1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Suppliers and Price of 1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

There total 2 articles about 1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53842-12-9
1-(p-chlorophenyl)-1,4-pentanedione

: 98909-44-5
1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / p-Me-C₆H₄-SO₃H / CCl₄ / Heating

2: 1.) Bu₄N(+) I(-), KOH, 2.) DCC, CuCl / 1.) THF, H₂O, r.t., 2.) THF, 20 h, reflux

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; copper(l) chloride; In tetrachloromethane;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 98909-39-8
1-(4-Chlorphenyl)-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

: 98909-44-5
1-(4-Chlorphenyl)-2-methylen-3-(2,4,5-trimethyl-1,3-dioxolan-2-yl)-1-propanon

Guidance literature:: With potassium hydroxide; tetra-(n-butyl)ammonium iodide; dicyclohexyl-carbodiimide; copper(l) chloride; Yield given. Multistep reaction; 1.) THF, H₂O, r.t., 2.) THF, 20 h, reflux;