bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

Base Information

Chemical Name:bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine
CAS No.:1067905-60-5
Molecular Formula:C₄₂H₄₇Br₂NSi
Molecular Weight:753.735
Hs Code.:

Synonyms:bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

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Technology Process of bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

There total 1 articles about bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 856219-73-3
acetic acid 1-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hept-2-ynyl ester

: 4316-58-9
tri(p-bromophenyl)amine

: 1067905-60-5
bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

Guidance literature:: tri(p-bromophenyl)amine; With n-butyllithium; In diethyl ether; for 4h; Cooling with ice;

With zinc(II) chloride; In diethyl ether; at 20 ℃; for 1h;

acetic acid 1-{2-[(triisopropylsilanyl)-ethynyl]-phenyl}-hept-2-ynyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; at -60 - 20 ℃;
DOI:10.1021/jo801689w

Reference yield: 83.0%

: 1067905-60-5
bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

: 1067905-65-0
bis(4-bromophenyl)-[4-((1E)-1-{3-[1-triisopropylsilanylmeth-(E)-ylidene]-3H-inden-1-yl}pent-1-enyl)phenyl]amine

Guidance literature:: In toluene; at 110 ℃; for 5h;
DOI:10.1021/jo801689w

Reference yield: 18.0%

: 1067905-60-5
bis(4-bromophenyl)-[4-(1-{2-[(triisopropyIsilanyl)ethynyl]phenylvinylidene}pentyl)phenyl]amine

: 1067905-69-4
bis(4-bromophenyl)(10-butyl-11H-benzo[b]fluoren-7-yl)-amine

: bis(4-bromophenyl)-[4-((1E)-1-{3-[1-triisopropylsilanylmeth-(Z)-ylidene]-3H-inden-1-yl}pent-1-enyl)phenyl]amine

: 1067905-65-0
bis(4-bromophenyl)-[4-((1E)-1-{3-[1-triisopropylsilanylmeth-(E)-ylidene]-3H-inden-1-yl}pent-1-enyl)phenyl]amine

Guidance literature:: With cyclohexa-1,4-diene; In toluene; at 17 ℃; for 6h; Temperature; Wavelength; Time; Reactivity; Photolysis; Inert atmosphere;
DOI:10.1021/jo801689w