2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline
CAS No.:77294-59-8
Molecular Formula:C₁₉H₂₄N₂O₄
Molecular Weight:344.411
Hs Code.:

Synonyms:2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

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Chemical Property of 2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

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Technology Process of 2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

There total 1 articles about 2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 76787-23-0
2-(2-amino-4,5-dimethoxyphenyl)-3,4-dihydro-6,7-dimethoxyquinoline

: 77294-59-8
2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; 1.) ice bath, 0.5 h 2.) room temperature, 4 h;
DOI:10.1002/jhet.5570170805

Reference yield: 21.0%

: 77294-59-8
2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

: 98-88-4
benzoyl chloride

: 77294-76-9
7-benzoyl-12,13-dihydro-6-hydroxy-2,3,9,10-tetramethoxy-6-phenyl-11bH-quino<1,2-c>quinazoline

Guidance literature:: for 2h; Heating;
DOI:10.1002/jhet.5570170805

Reference yield:

: 77294-59-8
2-(2-amino-4,5-dimethoxyphenyl)-6,7-dimethoxy-1,2,3,4-tetrahydroquinoline

: 77294-75-8
2-(2-formamido-4,5-dimethoxyphenyl)-6,7-dimethoxyquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / 0.5 h / Heating

2: 48 percent / 10percent aq. NaOH, DDQ / benzene / 5 h / Ambient temperature

With sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene;
DOI:10.1002/jhet.5570170805