tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

Base Information

Chemical Name:tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine
CAS No.:391611-15-7
Molecular Formula:C₂₀H₂₁NO
Molecular Weight:291.393
Hs Code.:

Synonyms:tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

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Chemical Property of tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

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Technology Process of tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

There total 2 articles about tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-64-9
tert-butylamine

: 176910-67-1
2-(4-methoxyphenylethynyl)benzaldehyde

: 391611-15-7
tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

Guidance literature:: at 20 ℃; for 24h;

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 391611-15-7
tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; 1percent CuI / 2percent PdCl₂(PPh₃)2 / 55 °C

With triethylamine; 2percent PdCl₂(PPh₃)2; 1: Sonogashira coupling;
DOI:10.1021/jo026016k

Reference yield: 89.0%

: C₁₆H₁₃IN₂⁽²⁺⁾*2CF₃O₃S^(1-)

: 391611-15-7
tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine

: C₂₂H₁₇INO⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: tert-Butyl-[1-[2-(4-methoxy-phenylethynyl)-phenyl]-meth-(E)-ylidene]-amine; With silver nitrate; In N,N-dimethyl acetamide; at 0 ℃; for 0.333333h;

C₁₆H₁₃IN₂⁽²⁺⁾*2CF₃O₃S^(1-); In N,N-dimethyl acetamide; at 20 ℃; for 3h;
DOI:10.1002/anie.201606381