(E)-6-phenylhex-2-enoic acid

Base Information

Chemical Name:(E)-6-phenylhex-2-enoic acid
CAS No.:84299-18-3
Molecular Formula:C₁₂H₁₄O₂
Molecular Weight:190.242
Hs Code.:

Synonyms:(E)-6-phenylhex-2-enoic acid

Suppliers and Price of (E)-6-phenylhex-2-enoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of (E)-6-phenylhex-2-enoic acid

Chemical Property:

Purity/Quality:

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Technology Process of (E)-6-phenylhex-2-enoic acid

There total 5 articles about (E)-6-phenylhex-2-enoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 6-Phenylhex-2-enoic acid t-butyl ester

: 84299-18-3
(E)-6-phenylhex-2-enoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1248/cpb.c15-00983

Reference yield: 69.0%

: 5581-75-9
6-phenylhexanic acid

: 84299-18-3
(E)-6-phenylhex-2-enoic acid

Guidance literature:: 6-phenylhexanic acid; With Zn(2,2,6,6-tetramethylpiperidine)_2*2LiCl; In tetrahydrofuran; at -40 ℃; for 1.5h; Inert atmosphere; Sealed tube;

With bis(η3-allyl-μ-chloropalladium(II)); Allyl acetate; In tetrahydrofuran; at -40 - 60 ℃; for 3h; diastereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201706893

Reference yield:

: 18328-11-5
3-benzyl propionaldehyde

: 84299-18-3
(E)-6-phenylhex-2-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 2.) THF

2: TFA / CH₂Cl₂

With sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm980567e