7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

Base Information

Chemical Name:7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol
CAS No.:137196-50-0
Molecular Formula:C₃₂H₄₀O₄
Molecular Weight:488.667
Hs Code.:

Synonyms:7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

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Chemical Property of 7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

Chemical Property:

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Technology Process of 7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

There total 1 articles about 7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6793-92-6
p-benzyloxyphenylbromide

: 13209-60-4
3β, 17β-diacetoxyandrost-5-ene-7-one

: 137196-52-2
7α-(4-benzyloxyphenyl)androst-5-ene-7β,17β-diol-3β-yl acetate

: 137196-51-1
7β-(4-benzyloxyphenyl)androst-5-ene-3β,7α,17β-triol

: 137196-50-0
7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

Guidance literature:: With 1,1-Dibromoethane; magnesium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, reflux, 1.5 h, 2.) THF, reflux, 10 h;
DOI:10.1016/0039-128X(91)90005-G

Reference yield: 62.4%

: 137196-50-0
7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

: 137196-57-7
7α-(4-hydroxyphenyl)androst-5-ene-3β,7β,17β-triol

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In methanol; under 2585.7 Torr;
DOI:10.1016/0039-128X(91)90005-G

Reference yield:

: 137196-50-0
7α-(4-benzyloxyphenyl)androst-5-ene-3β,7β,17β-triol

: 137196-58-8
7α-(4-(2-N,N-diethylaminoethoxy)phenyl)androst-5-ene-3β,7β,17β-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 62.4 percent / triethylamine, H₂ / Pd/C / methanol / 2585.7 Torr

2: 56 percent / K₂CO₃ / acetone / 20 h / Heating

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; acetone;
DOI:10.1016/0039-128X(91)90005-G