S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Base Information

Chemical Name:S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole
CAS No.:156385-61-4
Molecular Formula:C₃₃H₂₄Cl₂N₂O₇S
Molecular Weight:663.535
Hs Code.:

S<sup>2</sup>-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Synonyms:S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Chemical Property:

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Technology Process of S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

There total 4 articles about S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 19462-98-7
5,6-dichloro-2,3-dihydro-1H-1,3-benzodiazole-2-thione

: 156385-61-4
S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 12h; Ambient temperature;
DOI:10.1080/15257779408013253

Reference yield:

: 6306-39-4
1,2-dichloro-4,5-dinitrobenzene

: 156385-61-4
S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Raney Ni / ethanol / 4 h / Ambient temperature

2: 79 percent / aq. KOH / ethanol / 28.5 h / Heating

3: 92 percent / trimethylsilyl triflate / 1,2-dichloro-ethane / 12 h / Ambient temperature

With potassium hydroxide; trimethylsilyl trifluoromethanesulfonate; hydrogen; nickel; In ethanol; 1,2-dichloro-ethane;
DOI:10.1080/15257779408013253

Reference yield:

: 95-50-1
1,2-dichloro-benzene

: 156385-61-4
S²-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-mercapto-5,6-dichlorobenzimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / conc. HNO₃, H₂SO₄, SO₃ / 2 h / 100 °C

2: H₂ / Raney Ni / ethanol / 4 h / Ambient temperature

3: 79 percent / aq. KOH / ethanol / 28.5 h / Heating

4: 92 percent / trimethylsilyl triflate / 1,2-dichloro-ethane / 12 h / Ambient temperature

With potassium hydroxide; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sulfur trioxide; hydrogen; nitric acid; nickel; In ethanol; 1,2-dichloro-ethane;
DOI:10.1080/15257779408013253