ingenol 3-benzoate-20-trityl ether

Base Information

Chemical Name:ingenol 3-benzoate-20-trityl ether
CAS No.:256427-34-6
Molecular Formula:C₄₆H₄₆O₆
Molecular Weight:694.868
Hs Code.:

Synonyms:ingenol 3-benzoate-20-trityl ether

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Chemical Property of ingenol 3-benzoate-20-trityl ether

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Technology Process of ingenol 3-benzoate-20-trityl ether

There total 3 articles about ingenol 3-benzoate-20-trityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 65-85-0,8013-63-6
benzoic acid

: 79720-52-8
ingenol 20-trityl ether

: 256427-34-6
ingenol 3-benzoate-20-trityl ether

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at -18 ℃; for 12h;
DOI:10.1002/(SICI)1099-0690(199912)1999:12<3413::AID-EJOC3413>3.0.CO;2-S

Reference yield:

: 30220-46-3
ingenol

: 256427-34-6
ingenol 3-benzoate-20-trityl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DMAP / pyridine / 16 h

2: 45 percent / EDC; DMAP / CH₂Cl₂ / 12 h / -18 °C

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In pyridine; dichloromethane; 1: Etherification / 2: Acylation;
DOI:10.1002/(SICI)1099-0690(199912)1999:12<3413::AID-EJOC3413>3.0.CO;2-S

Reference yield:

: 76-83-5
trityl chloride

: 256427-34-6
ingenol 3-benzoate-20-trityl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DMAP / pyridine / 16 h

2: 45 percent / EDC; DMAP / CH₂Cl₂ / 12 h / -18 °C

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In pyridine; dichloromethane; 1: Etherification / 2: Acylation;
DOI:10.1002/(SICI)1099-0690(199912)1999:12<3413::AID-EJOC3413>3.0.CO;2-S