7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

Base Information

Chemical Name:7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione
CAS No.:28910-87-4
Molecular Formula:C₁₅H₉ClF₂N₂S
Molecular Weight:322.766
Hs Code.:

7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[<i>e</i>][1,4]diazepine-2-thione

Synonyms:7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

Chemical Property:

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Technology Process of 7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

There total 7 articles about 7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28910-86-3
1,3-dihydro-7-chloro-5-(2,6-difluorophenyl)-2H-1,4-benzodiazepin-2-one

: 28910-87-4
7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

Guidance literature:: With diphosphorus pentasulfide; In pyridine;

Reference yield:

: 372-18-9
1,3-Difluorobenzene

: 28910-87-4
7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; n-butyllithium / tetrahydrofuran; n-heptane; benzene

2: sodium hydroxide / hydrogenchloride; water

3: benzene

4: ammonia / dichloromethane; cyclohexane

5: pyridine; ethyl acetate

6: diphosphorus pentasulfide / pyridine

With hydrogenchloride; diphosphorus pentasulfide; sodium hydroxide; n-butyllithium; ammonia; In tetrahydrofuran; pyridine; hydrogenchloride; n-heptane; dichloromethane; cyclohexane; water; ethyl acetate; benzene;

Reference yield:

: 28910-82-9
2-acetamido-5-chloro-2',6'-difluorobenzophenone

: 28910-87-4
7-chloro-5-(2,6-difluoro-phenyl)-1,3-dihydro-benzo[e][1,4]diazepine-2-thione

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / hydrogenchloride; water

2: benzene

3: ammonia / dichloromethane; cyclohexane

4: pyridine; ethyl acetate

5: diphosphorus pentasulfide / pyridine

With diphosphorus pentasulfide; sodium hydroxide; ammonia; In pyridine; hydrogenchloride; dichloromethane; cyclohexane; water; ethyl acetate; benzene;