N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

Base Information

Chemical Name:N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea
CAS No.:177416-11-4
Molecular Formula:C₁₆H₃₁N₄OS
Molecular Weight:327.514
Hs Code.:

Synonyms:N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

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Technology Process of N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

There total 4 articles about N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 168335-24-8
4-isothiocyanatomethyl-2,2,3,5,5-pentamethylimidazolidine-1-oxyl

: 177416-11-4
N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

Guidance literature:: In diethyl ether; for 18h; Ambient temperature;
DOI:10.1016/0040-4020(96)00203-7

Reference yield:

: 93509-45-6
4-bromomethyl-2,2,3,5,5-pentamethylimidazolidine 1-oxyl

: 177416-11-4
N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / sodium azide / acetone; H₂O / 4 h / Heating

2: 65 percent / diethyl ether / 1 h / Heating

3: 92 percent / 1.5 h / Heating

4: 96 percent / diethyl ether / 18 h / Ambient temperature

With sodium azide; In diethyl ether; water; acetone;
DOI:10.1016/0040-4020(96)00203-7

Reference yield:

: 168335-20-4
4-azidomethyl-2,2,3,5,5-pentamethylimidazolidine-1-oxyl

: 177416-11-4
N-cyclohexyl-N'-(1-oxyl-2,2,3,5,5-pentamethylimidazolidine-4-yl)-methylthiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / diethyl ether / 1 h / Heating

2: 92 percent / 1.5 h / Heating

3: 96 percent / diethyl ether / 18 h / Ambient temperature

In diethyl ether;
DOI:10.1016/0040-4020(96)00203-7