1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene

Base Information

• Chemical Name: 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene
• CAS No.: 61165-98-8
• Molecular Formula: C₃₀H₃₆O₉
• Molecular Weight: 540.61
• Mol file: 61165-98-8.mol

Synonyms:1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene

Chemical Property of 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene

There total 2 articles about 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(3,4,5-trimethoxyphenyl)methanol (3840-31-1) → 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene (61165-98-8) + 1,2,3,5,6,7-hexamethoxy-9,10-dihydro-anthracene (26952-98-7) + C30H36O9 (1581303-11-8)

Guidance literature:

With Tonsil Actisil FF; In neat (no solvent); at 85 ℃; for 0.0833333h; under 750.075 Torr; Time; Temperature; Reagent/catalyst; Microwave irradiation;

DOI:10.3390/molecules181012820

Reference yield: 40.0%

(3,4,5-trimethoxyphenyl)methanol (3840-31-1) → 1,2,3,6,7,8,11,12,13-nonamethoxy-10,15-dihydro-5H-tribenzo cyclononene (61165-98-8) + 5,5'-(oxybis(methylene))bis(1,2,3-trimethoxybenzene) (68299-87-6) + <2'(3'',4'',5''-trimethoxybenzyl)(3',4',5'-trimethoxybenzyl)3,4,5-trimethoxybenzyl> ether + 2'<2'',(3''',4''',5'''-trimethoxybenzyl)3'',4'',5''-trimethoxybenzyl>3',4',5'-trimethoxybenzyl ether

Guidance literature:

In carbon disulfide; for 7h; Heating; in presence of bentonite-clay;

DOI:10.1016/S0040-4039(00)78187-1

upstream raw materials:

(3,4,5-trimethoxyphenyl)methanol