2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

Base Information

Chemical Name:2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride
CAS No.:85021-71-2
Molecular Formula:C₂₁H₂₇NO₂S₂*ClH
Molecular Weight:426.044
Hs Code.:

Synonyms:2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

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Chemical Property of 2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

Chemical Property:

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Technology Process of 2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

There total 5 articles about 2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.2%

: 85021-70-1
4-(2-methyl-2-phenylpropoxy)benzyl-2-methylthio-Δ₂-thiazoline

: 85021-71-2
2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 12h; Heating;
DOI:10.1248/cpb.30.3563

Reference yield:

: 62516-91-0,74401-63-1
ethyl 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionate

: 85021-71-2
2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 84.4 percent / NaN₃ / H₂O; dimethylsulfoxide / 0.17 h / 95 °C

2: 1.) LiAlH₄, 2.) oxalic acid / 1.) Et₂O, room temp., 1 h, 2.) EtOH

3: 1.) Et₃N / 1.) pyridine, ice cooling, 1 h, 2.) pyridine, ice cooling, overnight

4: 56.7 percent / thionyl chloride / diethyl ether / 1 h / 0 °C

5: 65.2 percent / 6N HCl / ethanol / 12 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; sodium azide; oxalic acid; triethylamine; In diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1248/cpb.30.3563

Reference yield:

: 345651-63-0
2-(N-dithiocarbomethoxy)-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propan-1-ol

: 85021-71-2
2-amino-3-<4-(2-methyl-2-phenylpropoxy)phenyl>propyl methyl dithiolcarbonate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 56.7 percent / thionyl chloride / diethyl ether / 1 h / 0 °C

2: 65.2 percent / 6N HCl / ethanol / 12 h / Heating

With hydrogenchloride; thionyl chloride; In diethyl ether; ethanol;
DOI:10.1248/cpb.30.3563