C₄₁H₄₆N₂O₈

Base Information

Chemical Name:C₄₁H₄₆N₂O₈
CAS No.:915225-37-5
Molecular Formula:C₄₁H₄₆N₂O₈
Molecular Weight:694.825
Hs Code.:

C<sub>41</sub>H<sub>46</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₄₁H₄₆N₂O₈

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Chemical Property of C₄₁H₄₆N₂O₈

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Technology Process of C₄₁H₄₆N₂O₈

There total 5 articles about C₄₁H₄₆N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 915225-36-4
C₂₀H₂₈N₂O₆

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 915225-37-5
C₄₁H₄₆N₂O₈

Guidance literature:: With pyridine; dmap; at 20 ℃;
DOI:10.1021/ja068707u

Reference yield:

: 915225-35-3
C₅₈H₅₆N₂O₆

: 915225-37-5
C₄₁H₄₆N₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: 190 mg / trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

2: 20 percent / pyridine / 4-dimethylaminopyridine / 20 °C

With pyridine; trifluoroacetic acid; dmap; In dichloromethane;
DOI:10.1021/ja068707u

Reference yield:

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 915225-37-5
C₄₁H₄₆N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: 50 percent / aq. H₂SO₄; KMnO₄ / 12 h / Heating

2.1: 99 percent / conc. H₂SO₄ / 60 h / Heating

3.1: 30 percent / NaBH₄ / methanol / 60 h / Heating

4.1: 30 percent / aq. HBr / 3.5 h / Heating

5.1: NaH / tetrahydrofuran / 3 h / Heating

5.2: tetrahydrofuran / 48 h / 30 °C

6.1: 190 mg / trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

7.1: 20 percent / pyridine / 4-dimethylaminopyridine / 20 °C

With pyridine; sodium tetrahydroborate; potassium permanganate; sulfuric acid; hydrogen bromide; sodium hydride; trifluoroacetic acid; dmap; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja068707u