3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

Base Information

Chemical Name:3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide
CAS No.:1443011-75-3
Molecular Formula:C₂₈H₂₅N₃O₄
Molecular Weight:467.524
Hs Code.:

Synonyms:3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

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Chemical Property of 3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

Chemical Property:

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Technology Process of 3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

There total 4 articles about 3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 98-01-1
furfural

: 1443011-81-1
C₁₈H₁₇N₃O₂

: 1443011-75-3
3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

Guidance literature:: With sodium cyanoborohydride; zinc(II) chloride; In methanol; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.04.036

Reference yield:

: 1019-52-9
4-hydroxy-3,5-dinitrobenzoic acid

: 1443011-75-3
3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; diisopropyl-carbodiimide; triethylamine / N,N-dimethyl-formamide / 48 h / 20 °C

2: tin(II) chloride dihdyrate / ethanol / 0.5 h / 80 °C

3: sodium cyanoborohydride; zinc(II) chloride / methanol / 1.5 h / 20 °C / Inert atmosphere

With tin(II) chloride dihdyrate; sodium cyanoborohydride; benzotriazol-1-ol; triethylamine; zinc(II) chloride; diisopropyl-carbodiimide; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.04.036

Reference yield:

: 1443011-78-6
4-hydroxy-N-(naphthalen-2-ylmethyl)-3,5-dinitrobenzamide

: 1443011-75-3
3,5-bis[(furan-2-ylmethyl)amino]-4-hydroxy-N-(naphthalen-2-ylmethyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethanol / 0.5 h / 80 °C

2: sodium cyanoborohydride; zinc(II) chloride / methanol / 1.5 h / 20 °C / Inert atmosphere

With tin(II) chloride dihdyrate; sodium cyanoborohydride; zinc(II) chloride; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.04.036