(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

Base Information

Chemical Name:(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine
CAS No.:198015-59-7
Molecular Formula:C₁₇H₂₃Br₂NO₂
Molecular Weight:433.183
Hs Code.:

Synonyms:(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

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Chemical Property of (S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

Chemical Property:

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Technology Process of (S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

There total 6 articles about (S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 198015-57-5
(S)-(-)-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

: 198015-59-7
(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 18h;
DOI:10.1016/S0040-4020(97)00988-5

Reference yield:

: 100-46-9
benzylamine

: 198015-59-7
(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent Turnov_. / dimethylsulfoxide / 20 h

2: 95 percent / K₂CO₃ / tetrahydrofuran / 18 h

With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(97)00988-5

Reference yield:

: 198015-55-3
(2S)-1,1-dibromo-2-bromomethyl-2-methylcyclopropane

: 198015-59-7
(S)-(+)-N-t-butoxycarbonyl-N-benzyl-2,2-dibromo-1-methylcyclopropylmethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent Turnov_. / dimethylsulfoxide / 20 h

2: 95 percent / K₂CO₃ / tetrahydrofuran / 18 h

With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(97)00988-5