Technology Process of C46H57N8O14Si(1+)*Cl(1-)
There total 10 articles about C46H57N8O14Si(1+)*Cl(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C45H54N8O14Si; methyl iodide;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 72h;
With
sodium chloride;
In
water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen; formic acid / ethyl acetate / 2068.65 - 2585.81 Torr / Catalyst
2: hydrogenchloride / acetonitrile
3: 1H-imidazole / Solvent
4: Alkaline conditions; Solvent
5: triethyl phosphite / Solvent; Reflux
6: 2,6-dimethylpyridine / triethyl phosphite; tris(dibenzylideneacetone)dipalladium(0) chloroform complex / N,N-dimethyl-formamide / 48 h / 20 °C
7: tetrahydrofuran / 72 h / 0 - 20 °C
With
1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; formic acid; hydrogen; triethyl phosphite;
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triethyl phosphite;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: Solvent; Heating; Alkaline conditions
2: hydrogen; formic acid / ethyl acetate / 2068.65 - 2585.81 Torr / Catalyst
3: hydrogenchloride / acetonitrile
4: 1H-imidazole / Solvent
5: Alkaline conditions; Solvent
6: triethyl phosphite / Solvent; Reflux
7: 2,6-dimethylpyridine / triethyl phosphite; tris(dibenzylideneacetone)dipalladium(0) chloroform complex / N,N-dimethyl-formamide / 48 h / 20 °C
8: tetrahydrofuran / 72 h / 0 - 20 °C
With
1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; formic acid; hydrogen; triethyl phosphite;
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triethyl phosphite;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;