methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside
CAS No.:1064045-12-0
Molecular Formula:C₅₀H₅₅NO₁₁
Molecular Weight:845.987
Hs Code.:

Synonyms:methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

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Technology Process of methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

There total 3 articles about methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1064045-05-1
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

: 128962-63-0,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-α-L-rhamanopyranoside

: 108-24-7
acetic anhydride

: 1064045-12-0
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside; ethyl 2,3,4-tri-O-benzyl-1-thio-α-L-rhamanopyranoside; With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In diethyl ether; at -60 ℃;

acetic anhydride; With acetic acid; at 55 ℃; for 18h; Further stages.;
DOI:10.1021/jo801117y

Reference yield: 64.0%

: 108-24-7
acetic anhydride

: 136758-06-0,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-rhamnopyranoside

: 496065-67-9
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1064045-12-0
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside; With 4 A molecular sieve; methyl trifluoromethanesulfonate; In diethyl ether; at 20 ℃; for 18h;

ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-rhamnopyranoside; In diethyl ether; at 20 ℃; for 18h;

acetic anhydride; With acetic acid; at 55 ℃; for 18h; Further stages.;
DOI:10.1021/jo801117y

Reference yield: 25.0%

: 1064045-05-1
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 136758-06-0,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-rhamnopyranoside

: 1064045-12-0
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside; ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-rhamnopyranoside; With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In diethyl ether; at -60 ℃;

acetic anhydride; With acetic acid; at 55 ℃; for 18h; Further stages.;
DOI:10.1021/jo801117y