methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside
CAS No.:1064045-05-1
Molecular Formula:C₂₄H₂₉NO₇
Molecular Weight:443.497
Hs Code.:

Synonyms:methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

There total 2 articles about methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 333-27-7
methyl trifluoromethanesulfonate

: 496065-67-9
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1064045-05-1
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo801117y

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 333-27-7
methyl trifluoromethanesulfonate

: 496065-67-9
methyl 2-acetamido-3-O-benzoyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1064045-05-1
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

: 1064045-07-3
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-ethylacetimido-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; at 20 ℃; for 18h; Title compound not separated from byproducts.;
DOI:10.1021/jo801117y

Reference yield: 80.0%

: 1064045-05-1
methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 113893-72-4
2,3,4-tri-O-acetyl-L-rhamnopyranosyl trichloroacetimidate

: 1064045-15-3
methyl 2-acetamido-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-3-O-benzoyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: methyl 3-O-benzoyl-6-O-benzyl-2-deoxy-2-methylacetimido-β-D-glucopyranoside; 2,3,4-tri-O-acetyl-L-rhamnopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -70 ℃; for 1h;

acetic anhydride; With acetic acid; at 55 ℃; for 18h; Further stages.;
DOI:10.1021/jo801117y