Technology Process of N-tert-butyloxycarbonylaminoisophthalimide
There total 1 articles about N-tert-butyloxycarbonylaminoisophthalimide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / tetrahydrofuran / 0.08 h / 20 °C
2: 82 percent / 1,3-dicyclohexylcarbodiimide / tetrahydrofuran / 1 h
With
dicyclohexyl-carbodiimide;
In
tetrahydrofuran;
1: Acylation / 2: Cyclization;
DOI:10.1021/jo000225s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; triethylamine / tetrahydrofuran / 1 h / Heating
2: 97 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 5 °C
3: 65 percent / methylhydrazine / tetrahydrofuran / 0 - 20 °C
With
acetic acid; triethylamine; triphenylphosphine; methylhydrazine; diethylazodicarboxylate;
In
tetrahydrofuran;
1: Isomerization / 2: Methylation / 3: dephthaloylation;
DOI:10.1021/jo000225s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; triethylamine / tetrahydrofuran / 1 h / Heating
2: 83 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 - 5 °C
3: 65 percent / methylhydrazine / tetrahydrofuran / 0 - 20 °C
With
acetic acid; triethylamine; triphenylphosphine; methylhydrazine; diethylazodicarboxylate;
In
tetrahydrofuran;
1: Isomerization / 2: Alkylation / 3: dephthaloylation;
DOI:10.1021/jo000225s
