C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I

Base Information

• Chemical Name: C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I
• CAS No.: 1015254-21-3
• Molecular Formula: C₂₁H₂₇N₂*I
• Molecular Weight: 434.363
• Mol file: 1015254-21-3.mol

Synonyms:C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I

Chemical Property of C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I

There total 2 articles about C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH⁽¹⁺⁾*I^(1-)=(C₅H(CH₃)4CH₂CH(C₆H₅)NCHCHN(CH₃)CH)I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,4-tetramethylfulvene (76089-59-3) → C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH(1+)*I(1-)=(C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH)I (1015254-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium

2: tetrahydrofuran / 50 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In tetrahydrofuran;

DOI:10.1039/c3dt52052h

Reference yield:

1-benzylimidazole (4238-71-5) → C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH(1+)*I(1-)=(C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH)I (1015254-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium

2: tetrahydrofuran / 50 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In tetrahydrofuran;

DOI:10.1039/c3dt52052h

Reference yield: 90.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + n-butyllithium (109-72-8,29786-93-4) + C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH(1+)*I(1-)=(C5H(CH3)4CH2CH(C6H5)NCHCHN(CH3)CH)I (1015254-21-3) → C21H26LiN2*C4H8O

Guidance literature:

at -60 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/adsc.201200389

upstream raw materials:

1-benzylimidazole

1,2,3,4-tetramethylfulvene