N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

Base Information

Chemical Name:N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester
CAS No.:79974-22-4
Molecular Formula:C₂₈H₂₈N₂O₇
Molecular Weight:504.54
Hs Code.:

Synonyms:N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

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Chemical Property of N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

There total 4 articles about N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1676-73-9,25014-27-1
L-glutamic acid γ-benzyl ester

: 66891-86-9
benzyl (4-(chlorocarbonyl)phenyl)(methyl)carbamate

: 79974-22-4
N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water;
DOI:10.1021/jm00344a018

Reference yield:

: 10541-83-0,937737-33-2
N-methyl-p-aminobenzoic acid

: 79974-22-4
N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 2 N NaOH / dioxane; H₂O / 0.5 h / 0 - 5 °C

2: 99 percent / SOCl₂ / benzene / 2 h / Heating

3: 68 percent / (i-Pr)2NEt / dioxane; H₂O

With sodium hydroxide; thionyl chloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; benzene;
DOI:10.1021/jm00344a018

Reference yield:

: 2528-30-5
4-<<(benzyloxy)carbonyl>methylamino>benzoic acid

: 79974-22-4
N-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-L-glutamic acid γ-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / SOCl₂ / benzene / 2 h / Heating

2: 68 percent / (i-Pr)2NEt / dioxane; H₂O

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; benzene;
DOI:10.1021/jm00344a018