3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

Base Information

Chemical Name:3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester
CAS No.:198027-53-1
Molecular Formula:C₂₀H₂₆O₃
Molecular Weight:314.425
Hs Code.:

Synonyms:3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

Chemical Property:

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Technology Process of 3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

There total 1 articles about 3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one

: 188851-24-3
(1R,2R,3S,5S)-3-Benzyl-6,6-dimethyl-bicyclo[3.1.1]heptan-2-ol

: 67-64-1
acetone

: 198027-53-1
3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

Guidance literature:: In toluene; at 120 ℃; for 2h;
DOI:10.1080/00397910008087342

Reference yield:

: 198027-53-1
3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

: (S)-3-Hydroxy-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

: (R)-3-Hydroxy-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

Guidance literature:: With sodium tetrahydroborate; manganese(ll) chloride; In methanol; at 0 ℃; for 0.166667h; Title compound not separated from byproducts;
DOI:10.1080/00397910008087342

Reference yield:

: 526-55-6,930395-07-6
2-(3-indole)-ethanol

: 198027-53-1
3-Oxo-butyric acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

: ((R)-1-Methyl-1,3,4,9-tetrahydro-pyrano[3,4-b]indol-1-yl)-acetic acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

: ((S)-1-Methyl-1,3,4,9-tetrahydro-pyrano[3,4-b]indol-1-yl)-acetic acid (1R,2R,3S,5S)-3-benzyl-6,6-dimethyl-bicyclo[3.1.1]hept-2-yl ester

Guidance literature:: With tin(IV) chloride; In tetrahydrofuran; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1016/S0040-4039(97)01658-4