Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P]

Base Information

• Chemical Name: Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P]
• CAS No.: 695202-97-2
• Molecular Formula: C₂₄H₂₀P*C₃₁H₃₉FeO₃S₃Si₄
• Molecular Weight: 1063.43

Synonyms:Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P]

Chemical Property of Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P]

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Technology Process of Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P]

There total 1 articles about Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(CO)3^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(CO)3][(C₆H₅)4P] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Fe(CH3Si(C6H3(Si(CH3)3)S)3)(C4H8O)(1-)*(C6H5)4P(1+)=[Fe(CH3Si(C6H3(S)(Si(CH3)3))3)(C4H8O)][(C6H5)4P] (695202-95-0) + carbon monoxide (201230-82-2) → Fe(CH3Si(C6H3(Si(CH3)3)S)3)(CO)3(1-)*(C6H5)4P(1+)=[Fe(CH3Si(C6H3(S)(Si(CH3)3))3)(CO)3][(C6H5)4P] (695202-97-2)

Guidance literature:

In tetrahydrofuran; soln. of Fe-comp. in THF treated with CO (1 atm) at -48°C for 1 h; concd., layered with Et2O at -48°C; elem. anal.;

DOI:10.1002/anie.200352916

Reference yield: 75.0%

Fe(CH3Si(C6H3(Si(CH3)3)S)3)(CO)3(1-)*(C6H5)4P(1+)=[Fe(CH3Si(C6H3(S)(Si(CH3)3))3)(CO)3][(C6H5)4P] (695202-97-2) → Fe(CH3Si(C6H3(Si(CH3)3)S)2OCC6H3S(Si(CH3)3))(CO)2(1-)*(C6H5)4P(1+)=[Fe(C29H39OS3Si4)(CO)2][(C6H5)4P]

Guidance literature:

In tetrahydrofuran; soln. of Fe-comp. in THF stirred at room temp. for 2 h; evapd. to dryness, residue recrystd. from THF/Et2O; elem. anal.;

DOI:10.1002/anie.200352916

upstream raw materials:

Fe(CH₃Si(C₆H₃(Si(CH₃)3)S)3)(C₄H₈O)^(1-)*(C₆H₅)4P⁽¹⁺⁾=[Fe(CH₃Si(C₆H₃(S)(Si(CH₃)3))3)(C₄H₈O)][(C₆H₅)4P]

carbon monoxide

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