4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

Base Information

Chemical Name:4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester
CAS No.:86767-90-0
Molecular Formula:C₁₇H₁₄Cl₂N₂OS
Molecular Weight:365.283
Hs Code.:

Synonyms:4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

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Chemical Property of 4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

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Technology Process of 4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

There total 3 articles about 4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2521-24-6
4-chlorobenzothioamide

: 86767-79-5
4-Chloro-N-(1-chloro-cyclopropyl)-benzamide

: 86767-90-0
4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 1h;
DOI:10.1002/ardp.19833160705

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 86767-90-0
4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Et₃N / tetrahydrofuran / 1 h

2: 72 percent / SOCl₂ / CHCl₃ / 1.) room temp., 30 min, 2.) 40 deg C, 5 min

3: 92 percent / Et₃N / tetrahydrofuran / 1 h

With thionyl chloride; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1002/ardp.19833160705

Reference yield:

: 86750-55-2
4-Chloro-N-(1-hydroxy-cyclopropyl)-benzamide

: 86767-90-0
4-Chloro-thiobenzimidic acid 1-(4-chloro-benzoylamino)-cyclopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / SOCl₂ / CHCl₃ / 1.) room temp., 30 min, 2.) 40 deg C, 5 min

2: 92 percent / Et₃N / tetrahydrofuran / 1 h

With thionyl chloride; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1002/ardp.19833160705