4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene

Base Information

• Chemical Name: 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene
• CAS No.: 1384933-47-4
• Molecular Formula: C₄₇H₆₄N₂S
• Molecular Weight: 689.105
• Mol file: 1384933-47-4.mol

Synonyms:4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene

Chemical Property of 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene

There total 1 articles about 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,6-diisopropylbenzenamine (24544-04-5) + 4,5-dibromo-2,7-di-tert-butyl-9,9-dimethylthioxanthene (888733-57-1) → 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene (1384933-47-4)

Guidance literature:

With palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 90 ℃; for 16h;

DOI:10.1039/c2dt30247k

Reference yield: 100.0%

1,2-dimethoxyethane (110-71-4) + 4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene (1384933-47-4) → Li2(DME)2[4,5-bis(2,6-diisopropylanilino)-2,7-di-tert-butyl-9,9-dimethylthioxanthene(2-)]

Guidance literature:

With n-butyllithium; In hexane; at -78 - 20 ℃; for 12h;

DOI:10.1039/c2dt30247k

upstream raw materials:

2,6-diisopropylbenzenamine

4,5-dibromo-2,7-di-tert-butyl-9,9-dimethylthioxanthene