Technology Process of 2-(4-fluorophenyl)propane-1,3-diazide
There total 5 articles about 2-(4-fluorophenyl)propane-1,3-diazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
N,N-dimethyl-formamide;
at 55 ℃;
for 24h;
DOI:10.1021/ol701720m
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 65 percent / LiAlH4 / diethyl ether / 24 h / 20 °C
2: 91 percent / pyridine / CH2Cl2 / 24 h / 20 °C
3: sodium azide / dimethylformamide / 24 h / 55 °C
With
pyridine; lithium aluminium tetrahydride; sodium azide;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol701720m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 91 percent / pyridine / CH2Cl2 / 24 h / 20 °C
2: sodium azide / dimethylformamide / 24 h / 55 °C
With
pyridine; sodium azide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol701720m
