2-(4-fluorophenyl)propane-1,3-diazide

Base Information

Chemical Name:2-(4-fluorophenyl)propane-1,3-diazide
CAS No.:957131-20-3
Molecular Formula:C₉H₉FN₆
Molecular Weight:220.209
Hs Code.:

Synonyms:2-(4-fluorophenyl)propane-1,3-diazide

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Chemical Property of 2-(4-fluorophenyl)propane-1,3-diazide

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Technology Process of 2-(4-fluorophenyl)propane-1,3-diazide

There total 5 articles about 2-(4-fluorophenyl)propane-1,3-diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957131-16-7
2-(4-fluorophenyl)propane-1,3-diyl dimethanesulfonate

: 957131-20-3
2-(4-fluorophenyl)propane-1,3-diazide

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 55 ℃; for 24h;
DOI:10.1021/ol701720m

Reference yield:

: 2965-90-4
diethyl 2-(4-fluorophenyl)malonate

: 957131-20-3
2-(4-fluorophenyl)propane-1,3-diazide

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / LiAlH₄ / diethyl ether / 24 h / 20 °C

2: 91 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

3: sodium azide / dimethylformamide / 24 h / 55 °C

With pyridine; lithium aluminium tetrahydride; sodium azide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol701720m

Reference yield:

: 204201-52-5
2-(4-fluorophenyl)propane-1,3-diol

: 957131-20-3
2-(4-fluorophenyl)propane-1,3-diazide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

2: sodium azide / dimethylformamide / 24 h / 55 °C

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol701720m