N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Base Information

Chemical Name:N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide
CAS No.:479203-54-8
Molecular Formula:C₂₅H₃₃N₃O₄
Molecular Weight:439.555
Hs Code.:

N<sup>α</sup>-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Synonyms:N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Chemical Property:

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Technology Process of N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

There total 3 articles about N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 65864-22-4
(S)-2-amino-3-phenylpropionamide hydrochloride

: 126312-57-0
N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanine

: 479203-54-8
N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jm061238m

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 479203-54-8
N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / triethylamine / dioxane; H₂O / 2 h / 20 °C

2: 98 percent / diisopropylethylamine; benzotriazol-1-yloxytrispyrrolidinophosphonium*PF₆ / dimethylformamide / 4 h / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm061238m

Reference yield:

: 103854-26-8
α-(S)-2',6'-dimethylphenylalanine

: 479203-54-8
N^α-tert-butyloxycarbonyl-2',6'-dimethyl-L-phenylalanyl-L-phenylalanylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / triethylamine / dioxane; H₂O / 2 h / 20 °C

2: 98 percent / diisopropylethylamine; benzotriazol-1-yloxytrispyrrolidinophosphonium*PF₆ / dimethylformamide / 4 h / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm061238m