2-(2,6-dinitrophenyl)acetic Acid

Base Information

Chemical Name:2-(2,6-dinitrophenyl)acetic Acid
CAS No.:37777-63-2
Molecular Formula:C₈H₆N₂O₆
Molecular Weight:226.145
Hs Code.:
DSSTox Substance ID:DTXSID901034192

Synonyms:2-(2,6-dinitrophenyl)acetic Acid;37777-63-2;Benzeneacetic acid, 2,6-dinitro-;2,6-Dinitrophenylacetic acid;SCHEMBL3535123;2-(2,6-dinitrophenyl)aceticAcid;DTXSID901034192;AKOS005090974;3W-0056

Suppliers and Price of 2-(2,6-dinitrophenyl)acetic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(2,6-dinitrophenyl)acetic Acid

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:226.02258592
Heavy Atom Count:16
Complexity:285

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)[N+](=O)[O-])CC(=O)O)[N+](=O)[O-]

Technology Process of 2-(2,6-dinitrophenyl)acetic Acid

There total 5 articles about 2-(2,6-dinitrophenyl)acetic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 86162-89-2
dimethyl (2,6-dinitrophenyl)malonate

: 37777-63-2
(2,6-dinitro-phenyl)-acetic acid

: 86162-90-5
methyl (2,6-dinitrophenyl)acetate

Guidance literature:: With perchloric acid; In acetic acid; for 1h; Yields of byproduct given; Heating;
DOI:10.1021/jo00163a006

Reference yield:

: 86162-90-5
methyl (2,6-dinitrophenyl)acetate

: 37777-63-2
(2,6-dinitro-phenyl)-acetic acid

: 141-78-6
ethyl acetate

Guidance literature:: With perchloric acid; In acetic acid; at 125 ℃; for 1.5h; Heating / reflux;

Reference yield:

: 606-21-3
1-chloro-2,6-dinitrobenzene

: 37777-63-2
(2,6-dinitro-phenyl)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.)DMF, 2.) 20 to 90 deg C, 2 h, 25 deg C, 16 h, to 10 deg C

2: 70percent perchloric acid / acetic acid / 1 h / Heating

With perchloric acid; potassium tert-butylate; In acetic acid;
DOI:10.1021/jo00163a006