2-(methylselanyl)benzonitrile

Base Information

• Chemical Name: 2-(methylselanyl)benzonitrile
• CAS No.: 24845-06-5
• Molecular Formula: C₈H₇NSe
• Molecular Weight: 196.11
• Mol file: 24845-06-5.mol

Synonyms:2-(methylselanyl)benzonitrile

Chemical Property of 2-(methylselanyl)benzonitrile

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-(methylselanyl)benzonitrile

There total 6 articles about 2-(methylselanyl)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

dimethyl diselenide (7101-31-7) + 3-aminoindazole (874-05-5) → 2-(methylselanyl)benzonitrile (24845-06-5)

Guidance literature:

With tert.-butylhydroperoxide; copper diacetate; In water; acetonitrile; at 40 ℃; for 18h; Sealed tube;

DOI:10.1039/c9cc05099j

Reference yield:

2-(methylseleno)benzoic acid (6547-08-6) → 2-(methylselanyl)benzonitrile (24845-06-5)

Guidance literature:

Multi-step reaction with 3 steps

1: nBuOCHCl₂

2: aq. NH₃

3: P₂O₅

With ammonium hydroxide; dichloromethyl n-butyl ether; phosphorus pentoxide;

Reference yield:

2-methylselenobenzoyl chloride (1442-04-2) → 2-(methylselanyl)benzonitrile (24845-06-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NH₃

2: P₂O₅

With ammonium hydroxide; phosphorus pentoxide;

upstream raw materials:

2-(methylseleno)benzoic acid

2-methylselenobenzoyl chloride

2,2'-diselanediyl-di-benzoic acid

anthranilic acid

Downstream raw materials:

1-(2-Methylselanyl-phenyl)-2-phenyl-ethanone

1-(2-Methylselanyl-phenyl)-2-phenyl-ethane-1,2-dione